{"id":199068,"date":"2025-06-11T10:51:00","date_gmt":"2025-06-11T02:51:00","guid":{"rendered":"http:\/\/www.htt.hk\/?p=199068"},"modified":"2025-06-11T10:51:00","modified_gmt":"2025-06-11T02:51:00","slug":"%e5%a4%a9%e7%84%b6%e9%85%b6-%e7%ba%b3%e7%b1%b3%e9%85%b6%e4%bb%bf%e7%94%9f%e6%9d%82%e5%90%88%e4%bd%93%e7%b3%bb-%e5%82%ac%e5%8c%96%e6%9c%a8%e8%b4%a8%e7%b4%a0%e9%99%8d%e8%a7%a3%e7%9a%84%e6%96%b0","status":"publish","type":"post","link":"https:\/\/www.htt.hk\/?p=199068","title":{"rendered":"\u5929\u7136\u9176-\u7eb3\u7c73\u9176\u4eff\u751f\u6742\u5408\u4f53\u7cfb\u2014\u50ac\u5316\u6728\u8d28\u7d20\u964d\u89e3\u7684\u65b0\u5de5\u5177"},"content":{"rendered":"\n<p>\u8fd1\u65e5\uff0c\u300a\u50ac\u5316\u5b66\u62a5\u300b\u5728\u7ebf\u53d1\u8868\u4e86\u897f\u5b89\u4ea4\u901a\u5927\u5b66\u8d39\u5f3a\u6559\u6388\u56e2\u961f\u5728\u6728\u8d28\u7d20\u964d\u89e3\u9886\u57df\u7684\u6700\u65b0\u7814\u7a76\u6210\u679c\u6587\u7ae0\u3002\u8be5\u5de5\u4f5c\u501f\u9274\u81ea\u7136\u754c\u964d\u89e3\u6728\u8d28\u7d20\u7684\u591a\u9176\u534f\u540c\u6a21\u5f0f\uff0c\u6784\u5efa\u4e86\u5929\u7136\u9176-\u7eb3\u7c73\u9176\u4eff\u751f\u6742\u5408\u4f53\u7cfb\uff0c\u6210\u529f\u5b9e\u73b0\u4e86\u6e29\u548c\u53cd\u5e94\u6761\u4ef6\u4e0b\u6728\u8d28\u7d20\u7684\u9ad8\u6548\u964d\u89e3\uff0c\u5e76\u663e\u8457\u63d0\u9ad8\u4e86\u82b3\u9999\u65cf\u5c0f\u5206\u5b50\u4ea7\u7269\u7684\u6bd4\u4f8b\u3002<\/p>\n\n\n\n<p>\u968f\u7740\u5316\u77f3\u8d44\u6e90\u7684\u65e5\u76ca\u67af\u7aed\uff0c\u5f00\u53d1\u53ef\u518d\u751f\u66ff\u4ee3\u8d44\u6e90\u5df2\u6210\u4e3a\u53ef\u6301\u7eed\u53d1\u5c55\u7684\u91cd\u8981\u9700\u6c42\u3002\u6728\u8d28\u7d20\u4f5c\u4e3a\u81ea\u7136\u754c\u50a8\u91cf\u6700\u4e30\u5bcc\u7684\u53ef\u518d\u751f\u82b3\u9999\u65cf\u805a\u5408\u7269\uff0c\u662f\u5408\u6210\u9ad8\u503c\u82b3\u9999\u5316\u5408\u7269\u7684\u7406\u60f3\u66ff\u4ee3\u539f\u6599\u3002\u7136\u800c\uff0c\u6728\u8d28\u7d20\u7ed3\u6784\u590d\u6742\u3001\u5f02\u8d28\u6027\u5f3a\uff0c\u5c06\u5176\u5b9a\u5411\u964d\u89e3\u4e3a\u82b3\u9999\u5c0f\u5206\u5b50\u9762\u4e34\u5de8\u5927\u6311\u6218\u3002\u81ea\u7136\u754c\u4e2d\u6728\u8d28\u7d20\u7684\u964d\u89e3\u901a\u5e38\u7531\u591a\u79cd\u5929\u7136\u9176\u534f\u540c\u5b8c\u6210\uff0c\u5177\u6709\u53cd\u5e94\u6761\u4ef6\u6e29\u548c\u3001\u73af\u5883\u53cb\u597d\u7b49\u4f18\u52bf\u3002<\/p>\n\n\n\n<p>\u4f46\u5929\u7136\u9176\u6784\u6210\u7684\u4f53\u5916\u591a\u9176\u4f53\u7cfb\u50ac\u5316\u6027\u80fd\u5e38\u4e0d\u5c3d\u4eba\u610f\uff0c\u5929\u7136\u9176\u7684\u86cb\u767d\u8d28\u6027\u8d28\u5982\u7535\u8377\u72b6\u6001\u3001\u4eb2\u758f\u6c34\u6027\u548c\u5c3a\u5bf8\u5927\u5c0f\u7b49\u53ef\u80fd\u9650\u5236\u4e86\u5b83\u4eec\u5bf9\u590d\u6742\u6728\u8d28\u7d20\u7279\u5b9a\u533a\u57df\u7684\u53ef\u53ca\u6027\u3002\u56e0\u6b64\uff0c\u5f00\u53d1\u80fd\u591f\u5728\u6e29\u548c\u6761\u4ef6\u4e0b\u9ad8\u6548\u964d\u89e3\u6728\u8d28\u7d20\u5e76\u5b9a\u5411\u751f\u6210\u82b3\u9999\u65cf\u5316\u5408\u7269\u7684\u65b0\u65b9\u6cd5\u5177\u6709\u91cd\u8981\u610f\u4e49\u3002<\/p>\n\n\n\n<p>\u501f\u9274\u81ea\u7136\u754c\u591a\u9176\u534f\u540c\u964d\u89e3\u6728\u8d28\u7d20\u7684\u6a21\u5f0f\uff0c\u6574\u5408\u4e86\u53cd\u5e94\u6761\u4ef6\u9ad8\u5ea6\u517c\u5bb9\u800c\u7406\u5316\u6027\u8d28\u4e0d\u540c\u7684\u5929\u7136\u9176\u4e0e\u7eb3\u7c73\u9176\uff0c\u6784\u5efa\u4e86\u534f\u540c\u964d\u89e3\u6728\u8d28\u7d20\u7684\u5929\u7136\u9176-\u7eb3\u7c73\u9176\u4eff\u751f\u6742\u5408\u4f53\u7cfb\u3002\u8be5\u4f53\u7cfb\u80fd\u591f\u5728\u6e29\u548c\u6761\u4ef6\u4e0b\u5b9e\u73b0\u6728\u8d28\u7d20\u7684\u964d\u89e3\uff0c\u83b7\u5f97\u66f4\u9ad8\u6bd4\u4f8b\u7684\u82b3\u9999\u5c0f\u5206\u5b50\u5316\u5408\u7269\uff0c\u4e3a\u6728\u8d28\u7d20\u7684\u964d\u89e3\u63d0\u4f9b\u4e86\u65b0\u5de5\u5177\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/1-6.png\"><img loading=\"lazy\" decoding=\"async\" width=\"650\" height=\"314\" src=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/1-6.png\" alt=\"\" class=\"wp-image-199069\" srcset=\"https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/1-6.png 650w, https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/1-6-300x145.png 300w\" sizes=\"auto, (max-width: 650px) 100vw, 650px\" \/><\/a><\/figure>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/2-5.png\"><img loading=\"lazy\" decoding=\"async\" width=\"683\" height=\"393\" src=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/2-5.png\" alt=\"\" class=\"wp-image-199070\" srcset=\"https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/2-5.png 683w, https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/2-5-300x173.png 300w\" sizes=\"auto, (max-width: 683px) 100vw, 683px\" \/><\/a><\/figure>\n\n\n\n<p>\u56fe1. \u03bb-MnO2\u7eb3\u7c73\u9176\u7684\u8868\u5f81(a) TEM\uff1b(b) SAED\uff1b(c) HRTEM\uff1b(d-g)\u5143\u7d20\u5206\u6790\uff1b(h) XRD\uff1b(i-j) XPS\uff1b(k-l)\u9176\u6d3b\u3002<\/p>\n\n\n\n<p>\u901a\u8fc7\u6c34\u70ed\u6cd5\u6210\u529f\u5408\u6210\u4e86\u03bb-MnO2\u7eb3\u7c73\u9176\uff0c\u901a\u8fc7\u900f\u5c04\u7535\u5b50\u663e\u5fae\u955c\uff08TEM\uff09\u3001\u9009\u533a\u7535\u5b50\u884d\u5c04\uff08SAED\uff09\u3001X\u5c04\u7ebf\u884d\u5c04\uff08XRD\uff09\u4ee5\u53caX\u5c04\u7ebf\u5149\u7535\u5b50\u80fd\u8c31\uff08XPS\uff09\u5bf9\u5176\u5f62\u6001\u7279\u5f81\u548c\u5316\u5b66\u6210\u5206\u8fdb\u884c\u4e86\u8868\u5f81\u3002\u9176\u6d3b\u6d4b\u5b9a\u7ed3\u679c\u8868\u660e\uff0c\u03bb-MnO2\u7eb3\u7c73\u9176\u5177\u6709\u7c7b\u6f06\u9176\u6d3b\u6027\uff0c\u9176\u6027\u8fbe95.2 U\/g\uff0c\u8868\u660e\u5176\u5177\u6709\u6f5c\u5728\u7684\u6728\u8d28\u7d20\u964d\u89e3\u80fd\u529b\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/3-5.png\"><img loading=\"lazy\" decoding=\"async\" width=\"656\" height=\"377\" src=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/3-5.png\" alt=\"\" class=\"wp-image-199071\" srcset=\"https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/3-5.png 656w, https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/3-5-300x172.png 300w\" sizes=\"auto, (max-width: 656px) 100vw, 656px\" \/><\/a><\/figure>\n\n\n\n<p>\u56fe2. \u4e0d\u540c\u4f53\u7cfb\u7684\u6728\u8d28\u7d20\u964d\u89e3\u6027\u80fd(a)\u964d\u89e3\u7387\uff1b(b)\u5206\u5b50\u91cf\u5206\u5e03\uff1b(c-f)\u8868\u9762\u5f62\u8c8c\u53d8\u5316\u3002<\/p>\n\n\n\n<p>\u6728\u8d28\u7d20\u964d\u89e3\u80fd\u529b\u8bc4\u4f30\u7ed3\u679c\u8868\u660e\uff0cCotA+\u03bb-MnO2\u6742\u5408\u4f53\u7cfb\u7684\u6728\u8d28\u7d20\u964d\u89e3\u7387\u8fbe\u523025.15%\uff0c\u8fdc\u9ad8\u4e8e\u4ec5\u542b\u6709\u6f06\u9176CotA\uff0815.32%\uff09\u6216\u03bb-MnO2\u7eb3\u7c73\u9176\uff0814.90%\uff09\u7684\u5355\u4e00\u50ac\u5316\u5242\u4f53\u7cfb\u3002\u7ecf\u6742\u5408\u4f53\u7cfb\u964d\u89e3\u540e\u6728\u8d28\u7d20\u805a\u5408\u7269\u5206\u6563\u6027\u6307\u6570\uff08PDI\uff09\u663e\u8457\u4e0b\u964d\uff0c\u8868\u9762\u53d8\u5316\u66f4\u4e3a\u663e\u8457\uff0c\u8868\u660e\u7eb3\u7c73\u9176-\u5929\u7136\u9176\u6742\u5408\u4f53\u7cfb\u5177\u6709\u66f4\u5f3a\u7684\u6728\u8d28\u7d20\u964d\u89e3\u80fd\u529b\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/4-3.png\"><img loading=\"lazy\" decoding=\"async\" width=\"680\" height=\"535\" src=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/4-3.png\" alt=\"\" class=\"wp-image-199072\" srcset=\"https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/4-3.png 680w, https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/4-3-300x236.png 300w\" sizes=\"auto, (max-width: 680px) 100vw, 680px\" \/><\/a><\/figure>\n\n\n\n<p>\u56fe3. \u4e0d\u540c\u50ac\u5316\u4f53\u7cfb\u7684\u4ea7\u7269\u5206\u6790(a) GC-MS \u56fe\u8c31\uff1b(b)\u8102\u80aa\u65cf\u548c\u82b3\u9999\u65cf\u4ea7\u7269\u7684\u5206\u5e03\uff1b(c)\u957f\u94fe\u8102\u80aa\u65cf\u7684\u6bd4\u4f8b\uff1b(d) S\u3001G\u548cH\u578b\u4ea7\u7269\u7684\u5360\u6bd4\u3002<\/p>\n\n\n\n<p>\u5929\u7136\u9176-\u7eb3\u7c73\u9176\u6742\u5408\u4f53\u7cfb\u4ea7\u7269\u4e2d\u82b3\u9999\u5c0f\u5206\u5b50\u6bd4\u4f8b\u9ad8\u8fbe48%\uff0c\u5206\u522b\u6bd4\u6f06\u9176CotA\u548c\u03bb-MnO2\u7eb3\u7c73\u9176\u7684\u5355\u4e00\u50ac\u5316\u5242\u4f53\u7cfb\u9ad841.2%\u548c118.2%\u3002\u6839\u636e\u4e09\u79cd\u50ac\u5316\u4f53\u7cfb\u7684\u4ea7\u7269\u5206\u5e03\u7ed3\u679c\u63a8\u6d4b\uff0c\u6f06\u9176CotA\u50ac\u5316\u7684\u7532\u6c27\u57fa\u5316\u6539\u53d8\u4e86\u82b3\u9999\u65cf\u4ea7\u7269\u6027\u8d28\uff0c\u963b\u788d\u4e86\u03bb-MnO2\u7684\u5f00\u73af\u4f5c\u7528\uff0c\u4f7f\u5f97\u6742\u5408\u4f53\u7cfb\u4e2d\u66f4\u591a\u7684\u82b3\u9999\u4ea7\u7269\u88ab\u4fdd\u7559\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/5-3.png\"><img loading=\"lazy\" decoding=\"async\" width=\"739\" height=\"486\" src=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/5-3.png\" alt=\"\" class=\"wp-image-199073\" srcset=\"https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/5-3.png 739w, https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/5-3-300x197.png 300w\" sizes=\"auto, (max-width: 739px) 100vw, 739px\" \/><\/a><\/figure>\n\n\n\n<p>\u56fe4. \u6728\u8d28\u7d20\u7ed3\u6784\u7684\u8868\u5f81(a)\u5085\u7acb\u53f6\u53d8\u6362\u7ea2\u5916\u5149\u8c31\uff1b(b-e\uff09\u6728\u8d28\u7d20\u8102\u80aa\u65cf\u542b\u6c27\u4fa7\u94fe\u533a\u57df\uff08\u03b4C\/\u03b4H 50-90\/2.5-6.0\uff09\u548c\uff08f-i\uff09\u82b3\u9999\u65cf\u533a\u57df\uff08\u03b4C\/\u03b4H 100-150\/5.5-8.0\uff09\u7684HSQC NMR \u56fe\u8c31\u3002<\/p>\n\n\n\n<p>FT-IR\u56fe\u8c31\u663e\u793a\uff0c\u76f8\u8f83\u4e8eCotA\u50ac\u5316\u4f53\u7cfb\u548c\u6742\u5408\u4f53\u7cfb\uff0c\u03bb-MnO2\u50ac\u5316\u4f53\u7cfb\u5728\u82b3\u9999\u73af\u5bf9\u5e94\u7684\u632f\u52a8\u533a\u57df\u5f3a\u5ea6\u6709\u6240\u51cf\u5f31\uff0c\u8868\u660e\u03bb-MnO2\u80fd\u6709\u6548\u7834\u574f\u82b3\u9999\u73af\uff1b\u800cCotA\u50ac\u5316\u4f53\u7cfb\u5728S\u578b\u7ed3\u6784\u5355\u5143\u5bf9\u5e94\u7684\u533a\u57df\u4fe1\u53f7\u589e\u5f3a\uff0cG\u578b\u7ed3\u6784\u5355\u5143\u533a\u57df\u4fe1\u53f7\u51cf\u5f31\uff0c\u9a8c\u8bc1\u4e86\u5176\u7532\u6c27\u57fa\u5316\u80fd\u529b\u30022D HSQC NMR\u7ed3\u679c\u5370\u8bc1\u4e86CotA\u50ac\u5316\u4f53\u7cfb\u3001\u03bb-MnO2\u50ac\u5316\u4f53\u7cfb\u548c\u6742\u5408\u4f53\u7cfb\u5404\u81ea\u964d\u89e3\u7684\u6728\u8d28\u7d20\u7684\u7279\u6027\u548c\u80fd\u529b\uff0c\u4e3a\u63a8\u6d4b\u7684\u6742\u5408\u4f53\u7cfb\u964d\u89e3\u6728\u8d28\u7d20\u7684\u673a\u5236\u63d0\u4f9b\u4e86\u8bc1\u636e\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/6-2.png\"><img loading=\"lazy\" decoding=\"async\" width=\"652\" height=\"287\" src=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/6-2.png\" alt=\"\" class=\"wp-image-199074\" srcset=\"https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/6-2.png 652w, https:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/6-2-300x132.png 300w\" sizes=\"auto, (max-width: 652px) 100vw, 652px\" \/><\/a><\/figure>\n\n\n\n<p>\u56fe5. (a)\u00b7O2-\u548c(b)\u00b7OH EPR\u56fe\u8c31<\/p>\n\n\n\n<p>\u7535\u5b50\u987a\u78c1\u5171\u632f\uff08EPR\uff09\u5149\u8c31\u5206\u6790\u53d1\u73b0\uff0cCotA\u50ac\u5316\u4f53\u7cfb\u5185\u00b7O2-\u7684\u542b\u91cf\u76f8\u5bf9\u8f83\u9ad8\uff0c\u800c\u03bb-MnO2\u50ac\u5316\u4f53\u7cfb\u5185\u00b7OH\u66f4\u4e3a\u4e30\u5bcc\uff1b\u5728\u6742\u5408\u4f53\u7cfb\u4e2d\uff0c\u00b7O2-\u4e0e\u00b7OH\u7684\u542b\u91cf\u5747\u76f8\u5bf9\u8f83\u9ad8\uff0c\u8fdc\u8fdc\u8d85\u8fc7\u4e86\u5355\u4e00\u50ac\u5316\u5242\u4f53\u7cfb\uff0c\u5929\u7136\u9176\u4e0e\u7eb3\u7c73\u9176\u7684\u6742\u5408\u53ef\u80fd\u4fc3\u8fdb\u4e86\u4e24\u8005\u7684\u4ea7\u751f\u548c\u76f8\u4e92\u8f6c\u5316\uff0c\u662f\u6742\u5408\u4f53\u7cfb\u80fd\u591f\u6728\u8d28\u7d20\u964d\u89e3\u7387\u663e\u8457\u63d0\u9ad8\u7684\u91cd\u8981\u539f\u56e0\u3002<\/p>\n\n\n\n<figure class=\"wp-block-image size-full\"><a href=\"http:\/\/www.htt.hk\/wp-content\/uploads\/2025\/06\/7-1.png\"><img loading=\"lazy\" decoding=\"async\" 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